tga66 - An Overview

The TGA body weight alter curve is proven in Determine one. The first fat loss phase is definitely the volatilization followed by A serious decomposition move. The spinoff of excess weight change curve in eco-friendly displays a peak where by the height max is at 427.seventy one ˚C. The MS details is collected throughout the overall TGA experiment. Ion currents and TGA mass loss are plotted as a functionality of temperature (see Determine 2). It's important to bear in mind the products of a TGA test are Usually decomposition items, and that's correct in these experiments also. Thus, the intention is to be aware of the thermal degradation goods of nylon 66. TGA-MS continually monitors the decomposition off gases being a function of your time and temperature. The degradation mechanism of the polymer molecules breaking on the C-N bond generates scaled-down polymer molecules Along with the same unit of bicarbonyl polymethylene fragments plus the fragments will stop working into carbon dioxide, carbon monoxide, water, and hydrocarbons [5].

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TGA-FTIR consistently displays the decomposition off gases as being a operate of your time and temperature, when GC/MS can separate the a number of off-gasoline products that arrive off at tga66 a single stage in time.

The degradation of nylon 66 With this Component of the analyze was also carried out with a TGA5500. The off-gas merchandise had been analyzed using a FTIR for the IR spectra in addition to a GC/MS with the MS Examination.

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